This system may be used for demonstrations and experiments with a large number of reaction processes such as:-
Main components comprise of:-
The devices are suitable for oxidation processes with oxygen or air e.g chlorination or bromation.Liquid-gas-phase reactors are available as blowing or bubble columns.
Reaction vessel: Cylindrical vessel or jacketed vessel made of Duran glass, nominal capacity 13 liters.
Heater : Tank coil or jacketed heater 0.45 m2.
Air distribution: Glass filter
Reflux cooler : Screw-flights heat exchanger 0.06 m2.
Thermostat : Heating output 3 KW.
These reactors are particularly suitable for demonstrations and experiments with the following processes:
The reactions can proceed at normal pressure or in vacuum.
Reaction vessels: Jacketed vessels, cylindrical vessels, spherical vessels, made of glass, nominal capacity 2,4,6 or 10 liter
Preliminary heating : Heating jacket(jacketed vessel) hood heater (spherical or cylindrical vessels)
Agitator: Rated output: 17…130 W
Torque: 8…60 Ncm.
Speed indicator, torque indicator.
Magnetic stirrer lock, rotating mechanical seal inclined blade or anchor stirrer.
Reflux condenser : Jacket condenser 0.2,0.3 or 0.6 m2. Made of glass.
Metering funnel : capacity 100, 250, 500 or 1000 ml.
The Pressure reactors have the possible capacities of 500mL, 1L, 1.5L
Reactor type: Double Walled and Triple Walled
Operating pressure :-1 bar g (full vacuum) to +12bar g(+1.2MPa)
Operating temperature : -90 deg C to +200 deg C
The system does not include overhead stirrer.
Please contact us for customized system.
The parts that come into contact with fluid are made of borosilicate glass 3.3, PTFE, and SS316 and perfluor.
Support Structure [Poly-carbonate sliding window, epoxy-coating]
The system does not include overhead stirrer circulator and chiller.
The automated laboratory units is compact and fully automated plant designed for scale-up, process optimization or full-scale production of small quantities. The process management system has a convenient graphical user interface under WINDOWS; it is graphic recipe driven and programmed, making the automated laboratory unit easy to operate.
Using weighing modules which operate to an accuracy of 0.1 grams precisely operating dosing pumps and easy-to-use recipe control, the automated laboratory unit produces the products you require in exact accordance with your indications, fully automatically, reproducibly and continuously. With the automated laboratory unit’s convenient process management system you have access to all the process data, so that you can display, for example temperature profiles and mass and energy balances or carry out further processing of the data using an EXCEL spreadsheet. For carrying out material balances convenient interfaces are available using , for example standard HPLC test vessels.
The automated laboratory unit can be expanded on a modular basis to the Miniplant. Using our extensive range of components ( e,g, falling film and thin film evaporators to handle sensitive products) the automated laboratory unit can grow to meet you requirements and specifications right up to the status of a complex and networkable Miniplant.
The automated laboratory unit quickly pays for itself. Several customers have reported amortisation in as little as half a year.
Miniplants can be used to set up complete production units on a small scale. Miniplants are thus ideal for scale-up or the production of small quantities, for example in the production of active substances. For production conforming to GMP we develop plants to our customers specific requirements.
Central chemical storage (e.g. drums)
Miniplants are highly automated plants, which grow to meet the customer’s requirements. These plants equipped with the hardware and software components, provide a high performance and expandable process management system offering a high degree of user convenience. The Mini-plants expandable support structure provides significant performance and system reserves to cater for the possible incorporation of further systems. Mini-plants can be operated from any location with Ethernet-networked PCs.
The prinicipal features of the standard and applications software are: